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ACQUITY UPLC BEH Phenyl Column

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更新時間:2024-02-11 18:16:22瀏覽次數:109

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三鍵鍵合的苯己基配體、分析含有芳香環的化合物。

詳細介紹

ACQUITY UPLC BEH苯基柱含有一個三鍵鍵合的苯己基配體,與其他苯基色譜柱相比,它提供了行業的pH穩定性、批次重現性和優異的峰形。它設計用于提供相對于直鏈烷烴柱互補的選擇性,特別是對于那些含有芳香環的分析物。


Simultaneous determination of 12 illicit drugs in whole blood and urine by solid phase extraction and UPLC–MS/MS


A rapid and sensitive method based on solid phase extraction and ultra performance liquid chromatography–electrospray ionization tandem mass spectrometry (UPLC–ESI-MS/MS) for the simultaneous determination of amphetamine, methamphetamine, 3,4-methylenedioxyamphetamine, 3,4-methylene-dioxymethamphetamine, N-methyl-1-(3,4-methyl-enedioxyphenyl)-2-butanamine, 3,4-methylenedioxyethylamphetamine, p-methoxymethamphetamine, ephedrine, N-methylephedrine, cathinone, methcathinone, and ketamine in whole blood and urine was developed and validated. Following solid phase extraction, the analytes were separated on ACQUITY UPLC BEH Phenyl column (100 mm × 2.1 mm, 1.7 μm) under gradient elution using a phase containing of acetonitrile and 0.3% formic acid in water at a flow rate of 0.4 mL min?1 and analyzed by a triplequadrupole mass spectrometer in the multiple reaction monitoring (MRM) mode. The proposed method was linear for each analyte with correlation coefficients over 0.99. Recovery validation studies showed accuracy bias below 4.4%. Acceptable precision was also obtained with a relative standard deviation below 8.9%. The sensitivity of the assay was found to be adequate for the quantitation of the illicit drugs in whole blood and urine sample and was higher than reported methods. The present method was proved to be reliable and robust for drug screening in forensic toxicological analysis.

品名

編號

ACQUITY UPLC BEH Phenyl Column, 130?, 1.7 µm, 2.1 mm X 100 mm, 3/pkg

176000908

ACQUITY UPLC BEH Phenyl Column, 130?, 1.7 µm, 1 mm X 150 mm, 3/pkg

176001047

ACQUITY UPLC BEH Phenyl Column, 130?, 1.7 µm, 2.1 mm X 150 mm, 1/pkg

186003378

ACQUITY UPLC BEH Phenyl Column, 130?, 1.7 µm, 1 mm X 100 mm, 1/pkg

186002883

ACQUITY UPLC BEH Phenyl Column, 130?, 1.7 µm, 2.1 mm X 150 mm, 3/pkg

176001051

ACQUITY UPLC BEH Phenyl Column, 130?, 1.7 µm, 2.1 mm X 100 mm, 1/pkg

186002885

ACQUITY UPLC BEH Phenyl Column, 130?, 1.7 µm, 2.1 mm X 30 mm, 1/pkg

186003911

ACQUITY UPLC BEH Phenyl Column, 130?, 1.7 µm, 1 mm X 50 mm, 3/pkg

176000905

ACQUITY UPLC BEH Phenyl Column, 130?, 1.7 µm, 1 mm X 100 mm, 3/pkg

176000906

ACQUITY UPLC BEH Phenyl Column, 130?, 1.7 µm, 1 mm X 50 mm, 1/pkg

186002882

ACQUITY UPLC BEH Phenyl Method Validation Kit, 130?, 1.7 µm, 2.1 mm X 100 mm, 3/pkg

186004052

ACQUITY UPLC BEH Phenyl Column, 130?, 1.7 µm, 2.1 mm X 75 mm, 1/pkg

186005607

ACQUITY UPLC BEH Phenyl Method Validation Kit, 130?, 1.7 µm, 2.1 mm X 50 mm, 3/pkg

186004050

ACQUITY UPLC BEH Phenyl Column, 130?, 1.7 µm, 2.1 mm X 50 mm, 3/pkg

176000907

ACQUITY UPLC BEH Phenyl Method Validation Kit, 130?, 1.7 µm, 2.1 mm X 150 mm, 3/pkg

186006022

ACQUITY UPLC BEH Phenyl Column, 130?, 1.7 µm, 3 mm X 150 mm, 3/pkg

176001809

ACQUITY UPLC BEH Phenyl Column, 130?, 1.7 µm, 2.1 mm X 30 mm, 3/pkg

176001311

ACQUITY UPLC BEH Phenyl Column, 130?, 1.7 µm, 3 mm X 50 mm, 3/pkg

176001807

ACQUITY UPLC BEH Phenyl Column, 130?, 1.7 µm, 3 mm X 100 mm, 3/pkg

176001808

ACQUITY UPLC BEH Phenyl Column, 130?, 1.7 µm, 3 mm X 30 mm, 3/pkg

176001806

ACQUITY UPLC BEH Phenyl Column, 130?, 1.7 µm, 3 mm X 75 mm, 1/pkg

186005612

ACQUITY UPLC BEH Phenyl Method Validation Kit, 130?, 1.7 µm, 3 mm X 100 mm, 3/pkg

186004698

ACQUITY UPLC BEH Phenyl Column, 130?, 1.7 µm, 2.1 mm X 50 mm, 1/pkg

186002884

ACQUITY UPLC BEH Phenyl VanGuard Pre-column, 130?, 1.7 µm, 2.1 mm X 5 mm, 3/pkg

186003979

ACQUITY UPLC BEH Phenyl Method Validation Kit, 130?, 1.7 µm, 3 mm X 50 mm, 3/pkg

186004697

ACQUITY UPLC BEH Phenyl Column, 130?, 1.7 µm, 3 mm X 30 mm, 1/pkg

186004671

ACQUITY UPLC BEH Phenyl Column, 130?, 1.7 µm, 3 mm X 150 mm, 1/pkg

186004674

ACQUITY UPLC BEH Phenyl Column, 130?, 1.7 µm, 3 mm X 50 mm, 1/pkg

186004672

ACQUITY UPLC BEH Phenyl Column, 130?, 1.7 µm, 3 mm X 100 mm, 1/pkg

186004673


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